The Gladysz Research Group

Intragroup: Handouts

Administration:

- Campus Emergency Information Quick Reference Tool [pdf]

- Group Duty List [pdf]

- Group policies [pdf]

"How To" Series:

- How to make a publication box [pdf]

- How to find a chemical [pdf]

- Checking into the JAG group [pdf]

- Labeling Samples [pdf]

- Standardizing Alkyl Lithium Reagents [pdf]

- Melting point and describing solids [pdf]

- Characterizing Solid Compounds by DSC and TGA [pdf]

- Reporting Signifigcant Digits [pdf]

-------Rounding Numbers [pdf]

- Boiling point, pressure, manostat

------- Units of pressure [pdf]

------- boiling point vs. pressure 1 [pdf]

------- boiling point vs. pressure 2 [pdf]

------- how to use a manostat [pdf]

- Internal Standards [pdf]

- Solvates [pdf]

- Perchlorate Hazards [pdf]

- R/S Rules, Chiral Rhenium [pdf]

- X-ray reports

------- x-ray guidelines [pdf]

------- how to make an ORTEP plot [pdf]

------- useful x-ray references [pdf]

------- history of SHELX [pdf]

------- structure reports online [pdf]

- Tips for x-rays, crystals

------- tips to get crystals [pdf]

------- crystallization in the laboratory [pdf]

- Mass Spectrometry [pdf]

- Solvent Purification

------- NMR solvent data

-------------- cambridge [pdf]

------- -------euriso-top [pdf]

------- Water in solvents, useful citations [1] [2] [3] [4] [5][6]

--------CDFCl₂ preparation [pdf]

--------Determining peroxides in solvents[pdf]

--------Oxygen scavenging [pdf]

- Extractions [pdf]

Group Equipment:

- Glovebox procedures [pdf]

- UV-Vis procedures [pdf]

- IR Procedures [pdf]

- GC Procedures [pdf]

- HPLC procedures [pdf]

- CV procedures [pdf]

- Glassblowing procedures [pdf]

- Rotovap procedures [pdf]

- Microwave procedures [pdf]

- Solvent Purification procedures [pdf]

- Fischer-Porter bottles [pdf]

- Fischer-Porter bottles Ordering Information [pdf]

- Useful NMR chemical shifts [pdf]

- Making NMR reservations [pdf]

- Laboratory Safety Manual [Link]

- Chemical Storage Guidelines [pdf]